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YCN Newsletter 20 - Research in Spot by Emilija Nidžović
Synthesis, processing and characterization of high-entropy spinel oxides
Spinel oxides are metal oxides with the general formula AB2O4 and the spinel structure, where A and B represent different cations located at tetrahedral (A) and octahedral (B) sites. High-entropy spinel oxides (HESOs) contain five or more cations in these positions and have a single-phase crystal structure. These oxides have specific characteristics which make them suitable for a multitude of technological applications (e.g., catalysts, adsorbents, photocatalysts, sensors). Since the pioneering work of Dąbrowa and associates in 2018, various researchers have worked on the synthesis of HESOs, using different precursors and methods, as well as on investigating their properties.
My research focuses on synthesizing HESOs by utilizing the self-propagating room temperature (SPRT) method, which has not been used for this purpose in previous research. The main advantages of this approach are its time- and cost-effectiveness. Using it, I was able to synthesize single-phased high entropy spinel oxides of different compositions. After the synthesis, which produces samples in powder form, spark plasma sintering (SPS) is utilized in order to achieve densification. The sintering process occurs very fast and results in high-density ceramics.
Further steps of my PhD research will include assessing the structural, mechanical, thermal, electrical, magnetic, and other properties of the synthesized and processed samples. The ultimate goal is to contribute to both theoretical understanding and practical application of these materials.
Emilija Nidžović
Department of Materials, Vinča Institute of Nuclear Sciences, National Institute of thе Republic of Serbia, University of Belgrade, Belgrade, Serbia
Last news
YCN Newsletter 32 - Expert opinion - Maria Paula da Silva Seabra - CICECO, University of Aveiro
Turning Waste into Raw Materials for the Ceramic Industry.
Waste materials were once seen as a burden but are increasingly being redefined as valuable resources for ceramic production. Through advances in materials engineering, waste can be used as secondary raw materials in the ceramic industry. This shift enables more circular and resource-efficient ceramic manufacturing systems.
YCN Newsletter 32 - Industry in Spot - Dr. Daniel Bomze - Lithoz
Implementing 3D-Printed Technical Ceramics in Regulated Medical Fields.
Bringing a new manufacturing technology into medicine requires far more than producing an impressive component. In highly regulated fields, innovation must be translated into repeatable processes, documented quality, reliable materials and, ultimately, evidence of clinical value. Lithoz has spent more than a decade building this bridge for Lithography-based Ceramic Manufacturing (LCM).
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